666
22
,
514.5nm,
1000–1800cm 1.
SOLVER
(
)
.
2
2.1
X
Y–4Q
X–ray
YG8
X
(2–5).,1#
5min
YG8
Co
;
,
,
XRD
(
(111)
)
18.49nm,
.2#
3#
15min20min
YG8
Co
,
60min
,2#
:WC
(CNT)
Co;3#
:WC
Co.4#
21#
XRD
Fig.2XRDpatternsofcarboncoatingonto1#sam-ple
surface
32#
XRD
Fig.3XRDpatternsofcarboncoatingonto2#sam-plesurface
:WC
(CNT)
Co.CuKα
,
;
,Co
CuKα
,
,
.
2.2
Raman1#
:
(1156cm 1)(1338cm 1)
(1584cm 1);
,
[11,12]
(
6).
2#
,
:
(CNT,G
1
1584cmD
1362cm 1
G1629cm 1)(1334cm 1),G ;
:
(CNT,G
1584cm 1 1D
1362cm 1G
1629cm),D
G
,G
,
)
43#
XRD
Fig.4XRDpatternsofcarboncoatingonto3#
sample
surface
54#
XRD
Fig.5XRDpatternsofcarboncoatingonto4#sam-plesurface