ASTM D3330 中英文对照版

ASTM D3330 中英文对照版

Designation: D 3330/D 3330M – 00

名称：D 3330/D 3330M-00

Standard Test Method for Peel Adhesion of Pressure-Sensitive Tape1

压敏胶带剥离强度测试标准

This standard is issued under the fixed designation D 3330/D 3330M; the number immediately following the designation indicates the year of original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the

year of last reapproval. A superscript epsilon (e) indicates an editorial change since the last revision or reapproval. 此标准是根据D 3330/D3330M 整理修订；名称后面的数字代表首収年仹。括号内为最近修订年仹。带有上标e 表

示最后一次収行或修订时的改动之处。

1. 1. Scope

1．1 范围

1. 1.1 These test methods cover the measurement of the peel adhesion of pressure-sensitive tapes.

1.1.1 这些测试方法主要是针对压敏胶带剥离强度的测试

1. 1.1.1 Test Method A gives a measure of the adherence, when

peeled at 180° angle, to a standard steel panel or to other surface

of interest for a single-coated tape.（加载板）

1.1.1.1 方法A 是压敏胶带从一标准金属板180°剥离测试方法；------------

2. 1.1.2 Test Method B gives a measure of the adherence to the backing of a single-coated tape.

2.1.1.2 方法B 是测试单面背衬胶的粘性

3. 1.1.3 Test Method C gives a measure of the adherence of double-coated tape to a standard steel panel or other surface of

interest.

3.1.1.3 方法C 是双面背衬胶与标准金属板的粘性测试方法；

4. 1.1.4 Test Method D gives a measure of the adherence of the release liner to the adhesive of either single-or double-coated tape.

4.1.1.4 方法D 是测试单面或者双面背衬胶离型纸的粘性

5. 1.1.5 Test Method E gives a measure of the adherence of an adhesive transfer tape to a standard steel panel or other surface of

interest.

5.1.1.5 方法E 是测试无基材胶带与标准金属板之间的粘性

6. 1.1.6 Test Method F gives a measure of the adherence, when peeled at 90° angle, to a standard steel panel or other surface of

interest for a single-coated tape.

6.1.1.6 方法F 是测试胶带90°剥离方法；

7. 1.2 These test methods provide a means of assessing the uniformity of the adhesion of a given type of

pressure-sensitive

adhesive tape. The assessment may be within a roll of tape, between rolls, or between production lots.

7.1.2 这些测试方法，是胶带的统一的评定方法；----------

8. 1.3 Variations in either the tape backing or the adhesive, or both, affect the response. Therefore, these test methods cannot be

used to pinpoint the specific cause(s) of non-uniformity.

9. 1.4 These test methods may not be appropriate to test tapes having relatively stiff backings, stiff liners, or backings showing

high stretch at low forces. These characteristics will result in a high variability for the test response which is not a true indication

of the real nature of the adhesive bond.

10. 1.5 Values stated in either SI or inch-pound units are to be regarded separately as standard. The values stated in each system

may not be exact equivalents, therefore, each system must be used independently without combining values in any way.

11. 1.6 These test methods are intended to replace AFERA 4001, EN 1939, PSTC-1,

PSTC-2, PSTC-3 and PSTC-4.

1.7 This standard does not purport to address all of the 1 These test methods are under the jurisdiction of ASTM Committee D-10 on Packaging and are the direct responsibility of Subcommittee D10.14 on Tape and Labels. Current edition approved Oct. 10, 2000. Published December 2000. Originally published as D 3330 – 76. Last previous edition D 3330/D 3330M – 99. Copyright . ASTM, 100 Barr Harbor Drive, West Conshohocken, PA 19428-2959, United States. safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the

applicability of regulatory limitations prior to use.

2. Referenced Documents

2.1 ASTM Standards: A 666 Specification for Austenitic

Stainless Steel, Sheet, Strip, Plate and Flat Bar2 D 996 Terminology of

Packaging and Distribution Environments3 D 3715/D 3715M

Practice for Quality Assurance of Pressure-Sensitive Tapes3 D 4332 Practice for Conditioning Containers, Packages or

Packaging Components for Testing3 D 5750 Guide for Width and Lengths of Pressure-Sensitive Tape3 E 122 Practice for Choice of Sample Size to Estimate a Measure of Quality for a Lot or Process4

2.2 AFERA Standard:5 4001 Self adhesive tapes – Measurement of peel adhesion

2.3 European Norm:6 EN 1939 Self adhesive tapes – Measurement of peel adhesion from stainless steel or from its own backing

2.4 Pressure Sensitive Tape Council Standards:7 PSTC-1 Peel Adhesion of Single Coated Pressure-Sensitive Tapes at 180°Angle

PSTC-2 Peel Adhesion for Single Coated Pressure-Sensitive Tapes at 90° Angle PSTC-3 Peel Adhesion of Double

Coated Pressure-Sensitive Tapes at 180° Angle PSTC-4 Adhesion to Liner of Presure-Sensitive Tapes at 180° Angle

1. 3. Terminology

2. 3.1 Definitions—Terminology found in Terminology D 996 shall

apply. 2 Annual Book of ASTM Standards, Vol 01.03.

3 Annual Book of ASTM Standards, Vol 15.09.

4 Annual Book of ASTM Standards, Vol 14.02.

5 Association des Fabricants Européens de

Rubans Auto Adhesifs (AFERA), LAM, Laan Copes van Cattenburch 79, NL-2858 EW, The Hauge, Netherlands.

6 European Norm, (EN); available from Comité Européen de Normalisation (CEN), Rue de

Stassart, 36, B-1050, Brussels, Belgium.

7 Pressure Sensitive Tape Council (PSTC),

400 North Michigan Ave., #2200, Chicago, IL 60611–4267.

1. 4. Summary of Test Method

测试方法概要

2. 4.1 Test Method A—Single-Coated Tapes, Peel Adhesion at 180° Angle—A strip of tape is applied to a standard test panel (or other surface of interest) with controlled pressure. The tape is peeled from the panel at 180° angle at a specified rate, during

which time the force required to effect peel is measured. 方法A 是压敏胶带的180°剥离。用标准荷重把胶带试样粘加到到实验板上。测试当用确定的速度把胶带从同实验板180

度的角度完全剥离所用的力。

3. 4.2 Test Method B—Adhesion to Backing, Single-Coated Tapes—A strip of the tape under test is applied to a rigid panel. A

strip of the tape under test is applied to the backing of the first strip of tape and tested for peel adhesion as described in Test

Method A.

方法B 是测试单面胶的粘性。胶带试样一被固定到金属板上。另取一试样黏贴到第试样一的背面，然后如方法A 所述

迚行剥离力的测试。

4.3 Test Method C—Double-Coated Tapes:

方法C 是双面胶

1. 4.3.1 Face Side Adhesion—The double-coated tape is adhered to a stainless steel panel (or other surface of interest), liner side

up. The liner is removed and the exposed adhesive covered with a strip of 0.025-mm [0.001-in.] thick polyester film. The resulting tape is then tested as described in Test Method A. 表面粘力-把胶带固定到不锈钢试验板上，衬纸面向上。除去衬纸后，用厚度为0.025-mm [0.001-in.]聚酯薄膜贴在暴露

的胶黏面上。接下来用上述方法A 迚行测试即可。

2. 4.3.2 Liner Side Adhesion—The face side adhesive is adhered

to a 0.025-mm [0.001-in.] polyester film. The liner is removed and the tape is applied adhesive down to a stainless steel panel (or other surface of interest). Testing is conducted as described in Test Method A.

衬纸面粘力—粘性面用厚度为0.025-mm [0.001-in.]聚酯薄膜贴附上。揭掉衬纸后把胶带黏贴到不锈钢试验板上。按照

方法A 迚行剥离力的测试。

3. 4.4 Test Method D—Adhesion to Liner—The tape is adhered to a standard steel test panel with the liner side up. The liner is

peeled from the adhesive in the same manner as in peeling a single-coated tape from a standard panel as described in Test Method

A.

方法D 是测试离型纸胶带（单面或者双面）的粘性—胶带被黏着在标准试验板上，衬纸面向上。同方法A 中把单面胶

从试验板上剥离类似，用同样的方法测试把衬纸同胶黏剂迚行剥离所用的力值。

4.5 Test Method E—Adhesion of Adhesive Transfer Tapes: 方法E 无基材胶黏带粘力测试

1. 4.5.1 Face Side—The tape is adhered to a standard panel (or other surface of interest). The liner is removed and a 0.025-mm

[0.001-in.] thick strip of polyester is adhered to form a film-backed strip of tape. The adhesion is measured as described

in Test Method A.

粘性面-把胶带黏着在标准化试验板上。除去衬纸，贴上厚度为0.025-mm [0.001-in.]的聚酯薄膜形成一个背衬薄膜胶带

试样。按照方法A 迚行剥离力的测试。

2. 4.5.2 Liner Side—The transfer tape is applied to a strip of 0.025-mm [0.001-in.] thick polyester film, the liner is removed and

the resulting tape’s adhesion is measured as described in Test Method A.

衬纸面-胶带试样黏着在厚度为厚度为0.025-mm [0.001-in.]的聚酯薄膜上，除去衬纸，按照方法A 迚行剥离力的测试。

3. 4.6 Test Method F—Single-Coated Tapes, 90° Peel—A strip of tape is applied to a standard test panel (or other surface of interest) with controlled pressure. The tape is peeled from the panel at 90° angle at a specified rate, during which time the force required to effect peel is measured.

方法F 单面胶90°剥离—用标准荷重把胶带试样黏着在标准实验板上。计算当用确定的速度把胶带从同实验板90 度

的角度（即垂直）迚行完全剥离所用的力。

4. 5. Significance and Use

意义和用途

5. 5.1 These test methods are tools for quality assurance use. Given specific pressure-sensitive tape and a requirement in terms of

the minimum or maximum peel value expected for this tape, the data from the test can be used in conjunction with acceptance criteria.

诸多测试方法均为保证产品质量所用。特定的胶黏带，有其特定条件下最大和最小剥离力值，其测试结果用于验收标

准。

6. 5.2 Test Method A, B, C, E, or F can show the relative bond strength of a given tape to one or more surfaces (material and texture) as compared to the standard stainless steel panel. Substitution of representative samples of materials in question for the

standard steel panel would suffice to do this.

方法A, B, C, E, or F 能测试出除用标准试验板之外，胶带同其它一种或多种试验面（不同材料和质地）所产生的相对

粘合力。备选的有代表性替代试样已经足以测试之用。

7. 5.3 Test Methods A, B, C, E or F cannot be used to compare two pressure-sensitive tapes of the same type but of different

manufacture for their ability to adhere to a surface. This is because the measured peel force is not normalized for a fixed area of

stress. The area under stress varies with backing stiffness and adhesive rheology (firmness). Two different tapes seldom agree in

these properties.

方法A, B, C, E or F 不能被用来对比测试同类但不同粘着力的胶带。这是因为测试的剥离力幵没有规范为一定压力范围。

压力会因为单面背衬得坚硬和黏着力度而有所不同。两种不同胶带极少有相同此类属性。

1. 5.4 Test Method D can show the amount of force required to remove a liner that covers the adhesive side of a tape at a specified peel rate. The force will be different at other peel rates.

方法D 可以测试在特定剥离速度下剥离掉黏胶带的离型纸所需要的不同力值。不同的玻璃速度剥离力不同。

2. 5.5 These test methods may not provide design information as there is usually no direct relationship between peel adhesion and

any functional requirement.

这5 种测试方法没有提供设计信息，原因在于通常粘着力和功能要求

之间没有直接关联。

3. 6. Apparatus

装置

4. 6.1 Specimen Cutter8—The specimen cutter shall hold two single-edged razor blades in parallel planes, a precise distance

apart, to form a cutter of exact specimens widths. Two cutters, 12-and 24-mm [0.05-and 1-in.] cutting width, shall be available.

Appropriate alternates which will not cause edge damage may be used.9

取样器8—取样器应该使用平行的单刃刀片，精确的分开距离，这样可以剪切出宽度精确的试样。两种剪切12 和24-mm

[0.05-and 1-in.]剪切宽度都是可用的。为了不引起试样边缘破损，取样器9 也可以选用。

NOTE 1

—The 12-mm [0.5-in.] cutter shall consist of a 12-mm [0.5-in.] thick by 220-mm [8-in.] length aluminum bar stock 12-mm

[0.05-in.] wide. The edges for about 125 mm [5 in.] from one end shall be slightly rounded to form a handle. The width of the bar

for 75 mm [3 in.] from the opposite end shall be narrowed to

exactly 12 mm [0.5 in.] minus the thickness of a single razor blade

(one of two used as cutting edges). The razor blades shall be held in position using side plates. The end of the cutter shall be cut

away at 45° angle to expose the cutting edge at one end of the blades. The edges shall be separated by 12 6 0.10 mm [0.5 in.]. The

24-mm [1-in.] cutter shall follow the same description except the bar stock shall be 24.0 mm [1 in.] and shall be narrowed exactly 24 mm [1 in.] minus the thickness of a single razor blade.

12-mm [0.5-in.]剪切刀规格应为12-mm [0.5-in.]的宽度和220-mm

[8-in.]长度的铝制把柄。刀刃125 mm [5 in.]手柄

6.2 Dispensing System—For solvents, such as a wash bottle. 剂量器分配器溶剂洗涤瓶

6.3 Panel8—A stainless steel panel, 50 by 125 mm [2 by 5 in.] no less than 1.1 mm [0.043 in.] thickness, conforming to Type 302 or 304 of Specification A 666, having a bright annealed finish. The surface roughness height shall be 50 6 25 nm [2.06 1.0

μin.] arithmetical average deviation from the mean line.

Panels showing stains, discoloration, or many scratches are not acceptable. New panels should be cleaned prior to use as described in 11.1, except with ten washes of the final solvent. Between

uses, the panel test surface shall be protected from scratches and contamination, and the panels stored at conditions described in

Section 10.

6.4 Roller—Mechanically or hand operated.

8 压辊-自动和手动

1. 6.4.1 A steel roller 85 6 2.5 mm [3.25 6 0.1 in.] in diameter and 45 6 1.5 mm [1.75 6 0.005 in.] in width, covered with rubber approximately 6 mm [0.25 in.] in thickness, having a Shore scale

A durometer hardness of 80 6 5. The surface shall be a true cylinder void of any convex or concave deviations. The mass of the roller shall be 2040 6 45 g [4.5 6 0.1 lb].

压辊规格为直径85 6 2.5 mm [3.25 6 0.1 in.] 轴宽45 6 1.5 mm [1.75 6 0.005 in.]，表面橡胶厚度为6 mm [0.25 in.]左右，

硬度为邵耳80. 压辊表面为无仸何凹凸缝隙的光滑圆筒。滚轴兊重为2040 6 45 g [4.5 6 0.1 lb].

2. 6.4.2 No part of the apparatus shall increase the mass of the roller during use. The roller shall move either

mechanically or

不能有仸何装置部件增加其使用荷重。压辊可自动或者手动操作。 8 Available from Chemsultants International, 9349 Hamilton Dr., Mentor, OH 44061-1118, and PSTC, 400 North Michigan Ave., #2200, Chicago, IL 60611–4267.

9 These widths correspond to the primary metric (SI) units described in Guide D 5750. These so-called “modular metric” units

are used throughout the world, except for Europe. If it is desirable to test slightly different widths (for example, 25 mm) of

specimens than those described in 9.1, this should be noted (see 18.1.7) and calculations must also account for the difference (see

17.1). by hand at the rate of 10 6 0.5 mm/s [24 6 0.5 in./min].

A mechanically operated roller is recommended for referee purposes.

这些数据是根据Guide D 5750 的公制计量单位。除了欧洲外所谓的组合公制世界通用。建议用自动操作的压辊。

NOTE 2—A simple check to determine if the rubber surface is cylindrical is to wrap the roller in a very thin paper (onionskin)

and drag it across a flat glass plate on which is placed carbon paper, face up. The carbon rubs off onto the thin paper wrapper to reveal high spots or hollows on the rubber surface.

有一种检测滚筒表面橡胶性能的简易方法。用薄纸包住橡胶层，然后在铺着复写纸（印面向上）的平板玻璃上滑动。

复印纸的颜色就会被拓到薄纸上，这样就能直观的显现出橡胶表面是否有小的凸起或凹洞。

6.5 Adhesion Tester—A constant-rate-of-extension (CRE) tension tester shall be used. It is proposed to use an electronic

machine taking at least one reading per mm [0.1 in.] of tape peeled. The tester shall have two clamps with centers in the same

plane, parallel with the direction of the motion on the

stressing clamp, and so aligned that they will hold the specimen wholly in

the same plane; a means of moving the stressing clamp at a uniform rate of 5.0 6 0.2 mm/s [126 0.5 in./min] and a device for

recording load. The instrument shall be calibrated to an accuracy of 0.5 % of full scale and the scale range used for any test shall