ML-18_LCMS_24831_MedChemExpress

MedChemexpress(简称MCE)提供各信号通路及领域的数千种现货抑制剂、调节剂、激动剂及化合物分子库

File ..607 2017-06-07 12-05-47\BIZ2017-607-WYQ15.D Tgt Mass (CHM): Injection Date : 7 Jun 17 3:09 pm +0800 Seq. Line : 40 Sample Name : BIZ2017-607-WYQ15 Location : P1-F-08 Acq. Operator : CLJ_701 Inj : 1 Spec. Reported : MS Integration Inj Volume : 1 ul

Acq. Method : D:\chem32\1\DATA\20170607\20170607 2017-06-07 12-05-47\1-POS-3MIN.M Analysis Method : D:\CHEM32\1\DATA\20170607\20170607 2017-06-07 12-05-47\1-POS-3MIN.M Catalog No : HY-101844 Batch#24831 A-RP-186

Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA) Gradient: 5% to 95%B within 1.3 min Flow Rate :1.8ml/min

Column :SunFire C18, 4.6*50mm,3.5um A-RP-186 Oven Temperature : 45C

min

0.5

1 1.5

2 2.5mAU

250500

750 DAD1 B, Sig=214,4 Ref=off 0.818

1.4651

.4781.587

1.819

2.049

2.1092.2272.259

min

0.51

1.52

2.5mAU 0

2550

75 DAD1 C, Sig=254,4 Ref=off 0.814

1.669

1.819

2.049

2.389

min

0.51 1.5

2 2.50

10000

2000030000 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 70

2.084

min

0.5

1

1.5

2 2.50

5000

100001500020000 Ion 570.2, MSD1 570.2,Target Mass 569.2 +H Positive, EIC=569.9:570.9

2.083

Integration Results for DAD1 B, Sig=214,4 Ref=off

RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 0.82 0.02 2.99 2.06 0.21 ND 1.47 0.02 1.78 1.72 0.12 ND 1.48 0.01 0.38 0.69 0.03 ND 1.59 0.02 7.08 7.12 0.49 275 1.82 0.02 2.28 2.44 0.16 233 2.05 0.02 1403.27 1103.02 98.04 570 2.11 0.01 3.85 4.56 0.27 570 2.23 0.01 1.11 1.25 0.08 159 2.26 0.02 8.61 6.96 0.60 159

Integration Results for DAD1 C, Sig=254,4 Ref=off

RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 0.81 0.04 0.87 0.40 0.61 ND 1.67 0.02 0.32 0.29 0.22 ND 1.82 0.02 0.30 0.32 0.21 233 2.05 0.03 140.60 108.80 98.33 570 2.39 0.19 0.90 0.57 0.63 159

MS Report from Instrument: LCMS-02

LCMS-02 6/7/2017 16:10:42 CLJ_701Page 1 of 3